CLASS 9 Material Preparation Guide

Class 9: Metal Matrix Composites (MMCs)

Class 9 includes metal matrix composites (MMCs), which embed ceramic fibers or particles in a metal matrix. These materials are valued for combining the strength and wear resistance of ceramics with the ductility and toughness of metals. Common in military and high-performance sporting applications, MMCs offer tailored mechanical and thermal properties for demanding environments.

Hardness Range
Variable; soft matrix with hard inclusions
Typical Materials
Al-SiC, Ti-B₄C, Cu-Al₂O₃, Mg-SiC composites
Preparation Challenge
Particle Pull-Out & Polishing Relief

Material Categories

Particulate-Reinforced MMCs

Common Combinations
  • Aluminum + SiC
  • Magnesium + Al₂O₃
  • Copper + TiB₂
Key Features
  • Uniform particle distribution
  • Improved stiffness and wear resistance
  • Hard-soft interface issues during prep

Fiber-Reinforced MMCs

Examples
  • Aluminum + SiC fibers
  • Titanium + Boron fibers
  • Magnesium + Graphite fibers
Considerations
  • Anisotropic properties
  • Fiber orientation matters for analysis
  • Voids may form around fibers

High-Temperature MMCs

Common Systems
  • Ti-B₄C
  • Ni-SiC
  • Mo-Si₃N₄
Key Features
  • Thermal stability
  • Oxidation resistance
  • Polishing relief often severe

Preparation Guide

Key Preparation Challenges

Particle Pull-Out

Hard ceramic particles may dislodge during grinding and polishing, leaving voids or surface defects.

Polishing Relief

Disparity in hardness between matrix and reinforcement causes relief or surface unevenness.

Edge Rounding

Composites may lose edge definition due to differential wear across phases.

Void Retention

Microvoids or interfacial porosity must be preserved and not smeared during final polishing.

Recommended Preparation Steps

Sectioning

Use diamond wafering saws with coolant to avoid cracking ceramic reinforcements or matrix deformation.

Mounting

Vacuum impregnation helps support particles and fill interfacial voids for better edge retention.

Grinding

Use alumina or SiC papers. Apply minimal pressure and frequent rinsing to avoid particle pull-out.

Polishing

Diamond suspensions with low-nap cloths minimize relief. Final polish with colloidal silica can enhance phase contrast.

Quality Verification

Hard particles remain embedded with minimal pull-out

Polished surface shows minimal relief across phases

Interfaces and voids are clean and clearly defined

Edge features remain intact with no rounding