CLASS 8 Material Preparation Guide

Class 8: Hardened & Heat Treated Steels

Class 8 includes case-hardened, through-hardened, and tool steels—ferrous materials commonly used in structural, mechanical, and tooling applications. Their microstructures are influenced by alloying and thermal processing, resulting in enhanced hardness, wear resistance, and toughness. Tool steels often contain elements like vanadium and molybdenum and may reach Rockwell C hardness levels above 60.

Hardness Range
Rc 45–65 (varies by treatment)
Typical Materials
Tool Steels, Case Hardened Steels, Through-Hardened Steels
Preparation Challenge
Minimal; Ensure Edge Retention

Material Categories

Tool Steels

Common Grades
  • D2 (High Carbon, High Chromium)
  • M2 (High-Speed Steel)
  • O1 (Oil Hardened)
Key Features
  • Rc > 60 hardness
  • Alloying with Mo, V, Cr, Mn
  • Carbide distribution is critical

Case Hardened Steels

Common Methods
  • Carburizing
  • Nitriding
  • Carbonitriding
Key Features
  • Hard outer layer with tough core
  • Graded hardness profile
  • Requires cross-sectional polish

Through-Hardened Steels

Common Grades
  • 4140 Alloy Steel
  • 1080 High Carbon Steel
  • 52100 Bearing Steel
Preparation Notes
  • Uniform martensitic structure
  • Minimal surface relief
  • May contain retained austenite

Preparation Guide

Key Preparation Challenges

Edge Retention

Ensure specimen edges remain intact and sharp, especially when analyzing case depth or coating transitions.

Carbide Pull-Out

Hard carbides in tool steels may dislodge during polishing, leaving voids or relief.

Overetching

Excess etching can obscure grain boundaries or martensitic structures in hardened zones.

Phase Identification

Martensite, retained austenite, and carbides may require multiple etchants to differentiate clearly.

Recommended Preparation Steps

Sectioning

Use abrasive or diamond saws with coolant. Clamp firmly to avoid edge chipping or deformation.

Mounting

Compression mounting is suitable. For edge-sensitive applications, use edge retention mounting media.

Grinding

Use SiC or alumina with decreasing grit sizes. Maintain moderate pressure and clean thoroughly between steps.

Polishing

Diamond polishing followed by colloidal silica to reveal martensite and avoid relief in high-carbide regions.

Quality Verification

Martensite and carbides clearly resolved

Edge features retained and sharp

Minimal relief in hardened zones

No carbide pull-out or etching artifacts