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Kalling's No. 2

Material Specific

Composition

Ethyl alcohol 85–95%, Copper (II) chloride 0.5–5%, Hydrogen chloride 2–7%, Methyl alcohol 1–5%

PACE product, by weight

Method

Swab

Time

5–60 s

Alternative Names

Kallings 2Kalling's Reagent

Tags

stainless-steelaustenitic-stainlessduplex-stainlessnickel-alloy

Reveals

Grain boundaries in austenitic stainless steels; delta-ferrite in duplex; sigma phase (preferential boundary attack); carbides at boundaries

Typical Results

The standard etchant for austenitic stainless steels (304, 316, 321, 347), duplex (2205, 2507), and many nickel-base alloys. Reveals grain boundaries cleanly without attacking ferrite or matrix. Mild, and a good first-try etchant on austenitic SS.

Application Method

Method:Swab
Typical Time:5–60 s

Preparation Notes

PACE Kalling's No. 2 is supplied ready-to-use. Composition (by weight):

IngredientCAS No.%Hazardous
Ethyl alcohol64-17-585–95%Yes
Copper (II) chloride7447-39-40.5–5%Yes
Hydrogen chloride7647-01-02–7%Yes
Methyl alcohol67-56-11–5%Yes
Isopropyl alcohol67-63-01–5%Yes

Application Notes

Swab the freshly polished surface 5–60 s at room temperature. Rinse with water then ethanol; air-dry.

Troubleshooting

Sensitized 304/316 etches preferentially at boundaries; distinguish step vs ditch by morphology and confirm with 10% oxalic A262 Practice A. Cold-worked SS under-etches: extend to 60 s.

Storage Notes

Amber glass at room temperature. Stable several months.

Alternative Etchants

  • Adler's Etchant
  • Glyceregia
  • Vilella's Reagent (martensitic only)

Similar Etchants

  • Adler's Etchant

ASTM References

ASTM E407 #92ASTM A763